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The solution pH was measured with a Metrohm Aquatrode Plus combination electrode, filled with a saturated KCl/AgCl solution, and calibrated before each titration at the temperature in question using standard pH 4 and 7 buffers

Castilla-Cortzar I, Garca-Fernndez M, Delgado G, Puche JE, Sierra I, Barhoum R, Gonzlez-Barn S

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