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concentrations greater than 60 M were not tested due to known cytotoxic effects in 3T3-L1 cells

Retention times, full scans, and MS/MS spectra (for LC-QTOF-MS/MS) or diffractograms (for XRPD) were compared with those obtained from the analysis of reference standards or suitable databases such as PubChem, MassBank, or PDF-2, which are public repositories of mass spectra or commercial databases of diffraction patterns, respectively