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Methods A typical procedure for O -sulfation reaction To a 4 mL borosilicate vial equipped with a stir bar was added substrate (0.1 mmol, 1.0 equiv), Mn(OTf) 2 (3.6 mg, 0.01 mmol, 10 mol%), tetrabutylammonium 4-nitrophenyl sulfate ( n Bu 4 N-PNPS, 69.1 mg, 0.15 mmol, 1.5 equiv), and solvent (0.5 mL, c = 0.2 M)

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What If the Numbers Are Too High or Not Right